发明名称 METHOD OF PREPARING CONCENTRATE OF HIGHER POLYUNSATURATED FATTY ACID ETHYL ESTERS
摘要 FIELD: food industry. SUBSTANCE: concentrate is prepared by reesterification of cod-liver oil with fully anhydrous ethyl alcohol in presence of alkali catalyst, weight ratio of reactants being 1:(0.15- 0.4):(0.004-0.02), respectively. Reaction is carried out for 2-4 h at 14-20 C. Reaction mixture is the fractioned in presence of urea and alcohol at esters/urea/alcohol weight ratio 1:(2,0-3.0):(2.5-6.0), wherein urea complexes are crystallized at 14-20 C. Isolation of desired product is effected by single high-vacuum molecular distillation. EFFECT: improved purity of product, simplified preparation procedure, and reduced consumption of reagents. 2 cl, 3 ex
申请公布号 RU2209235(C2) 申请公布日期 2003.07.27
申请号 RU20000127781 申请日期 2000.11.08
申请人 BELOTSERKOVETS VIKTOR MIKHAJLOVICH;SIDOROV NIKOLAJ NIKOLAEVICH;BOEVA NEHLJA PETROVNA 发明人 BELOTSERKOVETS V.M.;SIDOROV N.N.;BOEVA N.P.;LUGOVAJA M.V.
分类号 C11B7/00;(IPC1-7):C11B7/00 主分类号 C11B7/00
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