发明名称 Manufacturing method of CdS photocatalyst for hydrogen production and method for producing hydrogen by use of the same
摘要 A method for preparing a CdS photocatalyst represented by general formula (I): m(a)/Cd[M(b)]S, comprising the steps of: dissolving Cd-containing and M-containing compounds in water in such an amount that the mol % of M ranges from 0.001 to. 20.00; adding one H2S or Na2S as a reactant in the solution with stirring to precipitate Cd[M]S; washing the precipitate with water and vacuum-drying the precipitate in a nitrogen environment at a temperature of 105~150° C. for 1.5~3.0 hours; doping a liquid m-containing compound to this precipitate in such an amount that the % by weight of m ranges from 0.10 to 5.00. In the formula, m represents a doped metal element as an electron acceptor selected from the group of Ni, Pd, Pt, Fe, Ru, Co or an oxidized compound of these metals; a represents a percentage by weight of m, ranging from 0.10 to 5.00; M is a promoter selected from the group consisting of V, Cr, Al, P, As, Sb and Pb; b represents mol % of M/(M+Cd), ranging from 0.001 to 20.00.
申请公布号 US6447650(B1) 申请公布日期 2002.09.10
申请号 US20010762293 申请日期 2001.02.07
申请人 KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY;CHONGGU CO., LTD. 发明人 PARK DAE-CHUL;BAEG JIN-WOOK
分类号 C01B3/04;B01J23/06;B01J23/80;B01J23/843;B01J27/04;B01J27/043;B01J27/049;B01J27/138;B01J27/14;B01J35/00;B01J35/02;C01B3/06;C01G11/02;(IPC1-7):C01B3/00;C01G9/00;C01G1/00 主分类号 C01B3/04
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