发明名称 METHOD FOR PRODUCING FLUORINATED ARYL METAL COMPOUND
摘要 PROBLEM TO BE SOLVED: To provide a method for producing a fluorinated aryl metal compound, with which an impurity-free fluorinated aryl metal compound such as bis(pentafluorophenyl)dialkyltin, etc., having a slight discoloration, can be simply and inexpensively produced and purified. SOLUTION: The fluorinated aryl metal compound is obtained by reacting a hydrocarbon magnesium halide with a halogenated fluoroaryl in a solvent containing an ether-based solvent to give a fluorinated aryl magnesium halide, and reacting the fluorinated aryl magnesium halide with an organometallic compound. Tin is more preferable as a metal atom contained in the organometallic compound. A chain-type ether solvent is preferable as the ether- based solvent, more concretely, diisopropyl ether, dibutyl ether and t-butyl methyl ether are more preferable. Preferably a magnesium halide being a by- product of the fluorinated aryl metal is precipitated and removed or treated with an acid.
申请公布号 JP2002226491(A) 申请公布日期 2002.08.14
申请号 JP20010362759 申请日期 2001.11.28
申请人 NIPPON SHOKUBAI CO LTD 发明人 IKENO IKUYO;MITSUI HITOSHI;IIDA TOSHIYA;MORIGUCHI TOSHIMITSU
分类号 C07F7/22;(IPC1-7):C07F7/22 主分类号 C07F7/22
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