发明名称 Preparation method of bis (alkylcyclopentadienyl) ruthenium
摘要 The present invention is a preparation method of the bis(alkylcyclopentadienyl)ruthenium by reacting a ruthenium compound, an alkylcyclopentadiene and a reducing agent, wherein the ruthenium compound, the alkylcyclopentadiene, and the reducing agent are reacted in the presence of a base. It is preferable that at least one of ammonia, amines, ammonium compounds, hydroxides, aniline, nitroaniline, aminophenol, aminodiphenyl, piperidine, Grignard reagents, alkali metals, alkoxides, phenyl lithium, methyl lithium, n-butyryl lithium, lithium aluminium hydride, and sodium amide is added as a base to the reaction system and the ruthenium compound, the alkylcyclopentadiene, and the reducing agent are reacted.
申请公布号 US2002064948(A1) 申请公布日期 2002.05.30
申请号 US20010804185 申请日期 2001.03.13
申请人 TANAKA KIKINZOKU KOGYO K.K. (JAPANESE CORPORATIN) 发明人 SAITO MASAYUKI;TANIUCHI JUN-ICHI
分类号 C07B61/00;C07F15/00;C07F17/02;C23C16/18;H01L21/3205;(IPC1-7):H01L21/443 主分类号 C07B61/00
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