发明名称 |
A method of making a calcium salt of 2-hydroxy-4-(mercaptomethyl)butanoic acid |
摘要 |
A method of making calcium-2-hydroxy-4-(mercaptomethyl)butanoate includes combining and mixing 2-hydroxy-4-(mercaptomethyl)butanoic acid and a calcium salt selected from calcium oxide and calcium hydroxide and water in a first reaction zone. The combining and mixing step is carried out over a first period of 3-120 seconds. The resulting reaction mixture is transferred at the end of the first period from the first reaction zone to a second reaction zone, the transferring step being carried out over a second period of 3-60 seconds. Heat generated by reaction between the 2-hydroxy-4-(mercaptomethyl)butanoic acid and the calcium salt in the second reaction zone is allowed to drive off sufficient water to produce a product mixture containing less than 5% (m/m) water. |
申请公布号 |
AU1260102(A) |
申请公布日期 |
2002.05.21 |
申请号 |
AU20020012601 |
申请日期 |
2001.11.07 |
申请人 |
TECHNICAL AND COMMERCIAL SERVICES INTERNATIONAL LIMITED |
发明人 |
ROGER GRAHAM DAKIN;SAREL WILHELMUS DU TOIT;RICHARD ALWYN HOUSEMAN;DAVID GEORGE STEDMAN |
分类号 |
C07C319/20;C07C323/52 |
主分类号 |
C07C319/20 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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