发明名称 Method for purifying tetrakis(fluoroaryl)borate compounds or tris(fluoroaryl)borate compounds
摘要 A solution containing an organic solvent and a compound including impurities, represented by, for example, general formula (1)(wherein R1 to R10 independently represent H, F, a hydrocarbon group or an alkoxy group, at least one of R1 to R5 is F, at least one of R6 to R10 is F, M is H, alkali metal, alkaline earth metal or alkaline earth metal halide, n is 3 or 4, and m is 2 when M is an alkaline earth metal, or m is 1 when M is the other) is mixed with water. The purified compound is reacted with a compound which forms a monovalent cation seed to prepare a derivative. Thus, a purifying method capable of efficiently and easily separating and removing colored components contained in tetrakis(fluoroaryl)borate compounds can be provided. Moreover, it is possible to provide a method capable of preparing a highly-pure tetrakis(fluoroaryl)borate derivative efficiently and at low costs.
申请公布号 US6281389(B1) 申请公布日期 2001.08.28
申请号 US19990391585 申请日期 1999.09.07
申请人 NIPPON SHOKUBAI CO., LTD. 发明人 MITSUI HITOSHI;IIDA TOSHIYA;IKENO IKUYO;HIRANO NAOKO;ARIYOSHI YUKIKO
分类号 C07F5/02;(IPC1-7):C07F5/02 主分类号 C07F5/02
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