发明名称 METHOD FOR PRODUCING N-HYDROCARBON OXYCARBONYLAMINO ACID
摘要 PROBLEM TO BE SOLVED: To provide a method for producing an N-hydrocarbon oxycarbonylamino acid, capable of obtaining a high-purity N-hydrocarbon oxycarbonylamino acid by a simple operation without passing through a complicated purification process and yet readily reusing a solvent. SOLUTION: This method for producing the N-hydrocarbon oxycarbonylamino acid comprises reacting an amino acid salt whose aqueous solution shows basicity with a dicarbonate compound in a mixed solution of a water-soluble organic solvent and water to give a reaction solution containing the salt of the N- hydrocarbon oxycarbonylamino acid as the objective substance, an alcohol and an N-hydrocarbon oxycarbonylamino acid ester as reaction by-products, removing the alcohol and the water-soluble organic solvent from the reaction solution, then extracting and removing the N-hydrocarbon oxycarbonylamino acid ester by using a water-insoluble organic solvent from the aqueous solution from which the alcohol and the water-soluble organic solvent are removed and bringing the aqueous solution containing the salt of the objective substance into contact with an acid.
申请公布号 JP2001114744(A) 申请公布日期 2001.04.24
申请号 JP19990295086 申请日期 1999.10.18
申请人 TOKUYAMA CORP 发明人 SHIIKI TAKAFUMI;HIROTA YOSHIHIRO;TANAKA KENJI
分类号 C07C269/04;C07C271/22;(IPC1-7):C07C269/04 主分类号 C07C269/04
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