发明名称 LIQUID CHROMATOGRAPH MASS SPECTROSCOPE
摘要 PROBLEM TO BE SOLVED: To provide effective information by arranging a mechanism mixing and introducing a part of eluted liquid from a plurality of columns into a single mass spectroscope and calculating purity in every collected sample by means of a signal from a mass spectroscope simultaneously in analysis by the mass spectroscope. SOLUTION: While proportioning valves 21, 22 are switched so as to vary a composition ratio between eluted liquids 3, 4, two pumps 11, 12 pressurize the liquids so as to feed them at a constant flow rate. A sample injector 5 is provided with a plurality of sample injection ports and high pressure flow passage switching valves for injecting the sample into a plurality of different flow passages. The injected sample is separated into unitary constituents by means of columns 61, 62 and each constituent of the eluted liquid is detected as a peak by means of a detector 7 having a plurality of detection flow passage. The solutions eluted from the columns 61, 62 are mixed together by a mixer 9 so as to be connected to a mass spectroscope 120 via a liquid chromatograph interface 110, and then, molecular weight information and structure information can be provided.
申请公布号 JP2000266738(A) 申请公布日期 2000.09.29
申请号 JP19990073156 申请日期 1999.03.18
申请人 HITACHI LTD;HITACHI SCI SYST LTD 发明人 ISHIZUKA TOSHIHIRO;YAMADA NORIAKI;TOMIOKA MASARU;NISHIDA TETSUYA;NAGAI SHINJI;DEGUCHI KISABURO
分类号 G01N27/62;G01N30/46;G01N30/72;G01N30/86;(IPC1-7):G01N30/72 主分类号 G01N27/62
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