发明名称 |
Process for making 2,4,6, 8,10,12- hexanitro- 2,4,6,8,10, 12- hexa azatetracyclo(5.5.0. 05,9.03,11} -dodecane |
摘要 |
In this process 2,6,8,12-tetraacetyl-2,4,6,8,10,12-hexaazatetracyclo-[5.5.0.05,903,11]-dodecane ("TADH") is subjected to nitrolysis in the presence of a mixed acid to form HNIW. The mixed acid comprises at least one nitronium ion source (preferably nitric acid) and at least one strong acid (preferably sulfuric acid) capable of generating a nitronium ion from the source. The ratio of nitronium ion source to strong acid and the amount of TADH used are selected so that, in the event that the nitrolysis reaction is carried out at 85° C., 99% nitramine conversion will occur within ten minutes. |
申请公布号 |
AU5585700(A) |
申请公布日期 |
2000.09.21 |
申请号 |
AU20000055857 |
申请日期 |
2000.02.15 |
申请人 |
CORDANT TECHNOLOGIES, INC. |
发明人 |
ANDREW JOHN SANDERSON;KIRSTIN WARNER;ROBERT B. WARDLE |
分类号 |
C07D487/22 |
主分类号 |
C07D487/22 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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