发明名称 PRODUCTION OF QUATERNARY AMMONIUM SALT GOOD IN SMELL STABILITY
摘要 PROBLEM TO BE SOLVED: To obtain the subject compound good in smell stability and useful as a substrate for fabric softeners, hair conditioners and the like by reacting a specific tertiary amine with a quaternizing agent in the presence of an antioxidizing agent or the like. SOLUTION: A tertiary amine of formula I A, B are each a 1-6C alkyl, a hydroxyalkyl or the like; D is a group of the formula: Cx H2x NHCOR<1> [R<1> is a 1-35C alkyl or an alkenyl; (x) is 2-6], a group of the formula: Cy H2y O-(YO)z - COR<1> [(y) is 2-6; Y is a 2-3C alkylene; (z) is 0-20]} (e.g. a compound of formula II) is reacted with a quaternizing agent preferably at 60-80 deg.C in the presence of an antioxidizing agent, a chelating agent or a quinone compound in an amount of 50-2,000 ppm based on the compound of formula I or III during or after the quaternization reaction to obtain the objective compound of formula III (E is a 1-4C alkyl or a hydroxyalkyl; X is an anion) (e.g. a compound of formula IV).
申请公布号 JPH11106366(A) 申请公布日期 1999.04.20
申请号 JP19970268398 申请日期 1997.10.01
申请人 KAO CORP 发明人 NISHIMOTO UICHIRO;KATO TORU
分类号 C07C209/82;C07C211/63;D06M13/02;D06M13/152;D06M13/322;D06M13/342;D06M13/345;D06M13/463;D06M101/12;(IPC1-7):C07C211/63 主分类号 C07C209/82
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