发明名称 |
METHOD FOR OBTAINING HEXAMETHYLENE DIAMINE FROM MIXTURES CONTAINING HEXAMETHYLENE DIAMINE |
摘要 |
The invention relates to a method for obtaining hexamethylene diamine (I) from a mixture (II) containing (I) hexamethylene diamine, (III) hexamethylenimine, (IV) a compound selected from the group consisting of 2-aminomethyl cyclopentylamine and 1,2-diaminocyclohexane, (V) an imine, and (VI) adipodinitrile and 6-aminocaproic acid nitrile. According to said method, (a) a mixture (II) is subjected to distillation, yielding (a1) a low-boiling fraction which essentially contains (III), (a2) a medium-boiling fraction (VII) containing (I), (IV) and (V), and (a3) a high-boiling fraction containing (V) and (VI); (b) a mixture (VII) is subjected to distillation, yielding (b1) an overhead which essentially contains (IV) and (b2) a mixture (VIII) containing (I) and (V) as bottom residue; and (c) a mixture (VIII) is subjected to distillation, yielding (c1) (I) as overhead and (c2) a bottom residue which contains the essential part of (V). |
申请公布号 |
WO9834903(A1) |
申请公布日期 |
1998.08.13 |
申请号 |
WO1998EP00506 |
申请日期 |
1998.01.30 |
申请人 |
BASF AKTIENGESELLSCHAFT;BASSLER, PETER;FISCHER, ROLF;LUYKEN, HERMANN;REHFINGER, ALWIN;VOIT, GUIDO |
发明人 |
BASSLER, PETER;FISCHER, ROLF;LUYKEN, HERMANN;REHFINGER, ALWIN;VOIT, GUIDO |
分类号 |
C07C209/84;C07C209/86;C07C211/12 |
主分类号 |
C07C209/84 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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