发明名称 |
PROCESS FOR PRODUCING -g(a)-HYDROXYIMINOPHENYLACETONITRILE. |
摘要 |
<p>A process for producing an alpha -hydroxyiminophenylacetonitrile represented by general formula [II], (wherein R<1>, R<2>, R<3> and Z are each as defined in the specification) by reacting a crude nitrile containing a phenylacetonitrile represented by general formula [I], (wherein R<1>, R<2>, R<3> and Z are each as defined in the specification) with an alkyl nitrite in the presence of a base, extracting the reaction mixture with water, and neutralizing the separated water layer with an acid. This process enables target alpha -hydroxyiminophenylacetonitriles to be readily produced in a highly pure form in high yield by extracting the reaction mass with water and neutralizing the separated water layer with an acid. <CHEM></p> |
申请公布号 |
GR3025916(T3) |
申请公布日期 |
1998.04.30 |
申请号 |
GR19980400085T |
申请日期 |
1998.01.15 |
申请人 |
SHIONOGI & CO., LTD.;SUMITOMO CHEMICAL COMPANY LIMITED |
发明人 |
TAKASE, AKIRA;KAI, HIROYUKI;MASUI, MORIYASU;MASUMOTO, KATUHISA;NAKAMURA, AKIHIKO;KIYOSHIMA, YUJIRO;SASAKI, MIKIO |
分类号 |
C07C251/48;C07C253/14;C07C253/30;C07C255/64;(IPC1-7):C07C255/62;C07C319/20;C07C323/63 |
主分类号 |
C07C251/48 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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