发明名称 PRODUCTION OF N-LONG-CHAIN ACYLAMINO ACID AND ITS SALT
摘要 PROBLEM TO BE SOLVED: To obtain an N-long chain-acylamino acid salt of high quality which is very useful as a surfactant of low irritation from inexpensive raw materials with industrial advantage by heating an aqueous solution containing a specific amidedinitrile and a specific basic substance. SOLUTION: An aqueous solution containing (A) an amidedinitrile of formula I (R is a 7-21 C hydrocarbon) and (B) a basic substance, for example, sodium hydroxide is heated to prepare an aqueous solution containing an amidenitrile of formula II, in addition, this aqueous solution is further heated to hydrolyze the compound of formula II in the presence of the component (B) to prepare the objective salt of formula III [M is a cation originating from the component (B)]. The component A is preferably prepared by reaction of an iminodinitrile of formula IV with a fatty acid halide of formula V (X is a halogen atom) in the presence the component B.
申请公布号 JPH09301941(A) 申请公布日期 1997.11.25
申请号 JP19960120288 申请日期 1996.05.15
申请人 KAWAKEN FINE CHEM CO LTD 发明人 FUJII TAMOTSU;KIN HIROSHI;KADO KAZUHIRO
分类号 B01J23/04;C07B61/00;C07C231/08;C07C231/12;C07C233/47;C07C233/49 主分类号 B01J23/04
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