| 摘要 |
The invention relates to a method for the production of a 2,2',4,4',6,6'-hexanitrostilbene (HNS) with specified purity and bulk density, generally referred to as HNS II, from a less pure raw-product with lower bulk density, generally referred to as HNS I. According to the invention, the raw-product is purified through recrystallisation from a solvent, of which N-methylpyrrolidone gives by far the best result, while the bulk density of the product is increased by ultrasonically treating the resulting crystals, thereby decreasing their length to bredth ratio.
|
