发明名称 |
PROCESS FOR THE MANUFACTURE OF N-PHOSPHONOMETHYLIMINODIACETIC ACID. |
摘要 |
<p>PCT No. PCT/GB94/00018 Sec. 371 Date Jul. 10, 1995 Sec. 102(e) Date Jul. 10, 1995 PCT Filed Jan. 6, 1994 PCT Pub. No. WO94/15939 PCT Pub. Date Jul. 21, 1994.A process for the manufacture of N-phosphonomethyliminodiacetic acid which comprises: 1) reacting iminodiacetic acid with phosphorous acid and a source of formaldehyde in aqueous solution in the presence of concentrated sulphuric acid; 2) filtering and recovering the N-phosphonomethyliminodiacetic acid product precipitated in stage (1); 3) recovering the filtrates from stage (2) and optionally removing a proportion of the water therefrom; 4) transferring the filtrates from stage (3) to a further reaction stage in which further iminodiacetic acid is reacted with phosphorous acid and a source of formaldehyde in the presence of sulphuric acid; and thereafter 5) repeating stages (1), (2), (3) and (4) in a plurality of re-cycles.</p> |
申请公布号 |
GR3023089(T3) |
申请公布日期 |
1997.07.30 |
申请号 |
GR19970400478T |
申请日期 |
1997.04.10 |
申请人 |
ZENECA LIMITED |
发明人 |
JONES, RAYMOND, VINCENT, HEAVON;STANDEN, MICHAEL, CHARLES, HENRY;RAE, GRAHAM, ANDREW;RITCHIE, DAVID, JOHN |
分类号 |
C07F9/38;(IPC1-7):C07F9/38 |
主分类号 |
C07F9/38 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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