发明名称 |
Process for refining crude fluoroalkylsulfonic acid with the use of water |
摘要 |
A process for refining a crude fluoroalkylsulfonic acid represented by the general formula RfSO3H wherein Rf is a fluoroalkyl group having 1 to 4 carbon atoms into a highly refined one substantially free of impurities, said process comprising the steps of: (a) providing said crude fluoroalkylsulfonic acid, (b) mixing said crude fluoroalkylsulfonic acid with water or said water and an active silica to obtain a mixture, (c) stirring said mixture while maintaining said mixture at a higher temperature than room temperature, and (d) subjecting the mixture treated in said step (c) to distillation.
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申请公布号 |
US5498754(A) |
申请公布日期 |
1996.03.12 |
申请号 |
US19940228872 |
申请日期 |
1994.04.18 |
申请人 |
CENTRAL GLASS CO., LTD. |
发明人 |
NAKAMURA, TAMIO;YOKOYAMA, TAKASHI;KOBAYASHI, YOSHIYUKI |
分类号 |
C07B63/00;C07C303/44;C07C309/04;C07C309/06;(IPC1-7):C07C309/04 |
主分类号 |
C07B63/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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