A process and device for vaporisation injections in equipments for gas chromatographic analysis.

摘要

The invention concerns a process and a device for splitless vaporizing injection of samples into equipments of gas chromatographic analysis. The technique is applied specially when liquid samples generate volumes of vapours which cannot be housed inside the vaporizing chamber. Inside the vaporisation chamber, kept at high temperature, evaporation of the sample solvent forms a cool zone where the solutes are retained while the solvent vapours expand out of the vaporizing chamber and leave the injector. The sample liquid is kept in place within the vaporization chamber by suitable obstacles or by a packing material. At the end of solvent evaportaion, i.e. when cooling ceases, the injection zone returns to the regulated injector temperature and the compounds to be analysed are transferred to the column by the carrier gas. <IMAGE>