摘要 |
C-8453/8412 PREPARATION OF DIARYL SULFONES Diaryl sulfones are formed in a two-stage procedure. The first involves the reaction of an aryl sulfonic acid with an aryl reagent containing active hydrogen while byproduct water is removed azeotropically. In the second stage, which contains unreacted sulfonic acid, is treated with a sulfone condensing agent and additional aryl reagent to react additional, unreacted aryl sulfonic acid from the first stage. |