摘要 |
Organic-swelled layered metal chalcogenides, e.g., titanometallates or silicotitanates, are intercalated with polymeric chalcogenide, e.g., polymeric silica by treatment with organic hydrolyzable polymeric chalcogenide precursor wherein hydrolysis to polymeric chalcogenide is enhanced by removal of organic hydrolysis by-products, during hydrolysis, e.g., by exposure of the reaction mixture to elevated temperatures. |