发明名称 PURIFICATION OF P-CUMYLPHENOL
摘要 PURPOSE:To obtain a compound useful as a raw material of germicide, nonionic surfactant or antioxidant in high purity, by stripping p-cumylphenol containing alpha-methylstyrene or phenol as an impurity under specific conditions. CONSTITUTION:p-Cumylphenol containing alpha-methylstyrene or phenol as impurity is subjected to stripping using an inert gas such as nitrogen and carbon dioxide and/or steam at 70-180 deg.C to provide p-cumylphenol. The stripping is carried out by batch type, continuous type, continuous countercurrent contact method, etc., introducing an inert gas or steam into a stirring vessel. A amount of the alpha-methylstyrene or phenol included in the p-cumylphenol is preferably <=10%, especially <=1%. Thus the aimed product having high purity is extremely effectively obtained in reduced decomposition of p-cumylphenol.
申请公布号 JPS63258440(A) 申请公布日期 1988.10.25
申请号 JP19870092321 申请日期 1987.04.15
申请人 MITSUBISHI PETROCHEM CO LTD 发明人 INABA MASASHI;KATAOKA MITSUGI
分类号 C07C37/14;C07C27/00;C07C37/70;C07C39/15;C07C67/00 主分类号 C07C37/14
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