发明名称 |
Method for producing bis [ beta (N,N-dimethylamino)ethyl]ether |
摘要 |
An improved process for preparing a bis [ beta -(N,N-dimethylamino)ethyl]ether by reacting a bismethohalide of bis [ beta -(N,N-dimethylamino)ethyl]ether represented by the following general formula: <IMAGE> (wherein X denotes a halogen atom), with an aliphatic amine having a boiling point of not lower than 220 DEG C. at atmospheric pressure and having a primary amino group in the molecule thereof. The process comprises the following two steps (a) and (b): (a) a step of distilling out water at a temperature of not more than 130 DEG C. under reduced pressure from a mixture of said bismethohalide aqueous solution and said aliphatic amine to provide a concentration of said bismethohalide to water of not less than 85% by weight, and (b) a step of reacting said bismethohalide and amine in a solid-liquid phase at a temperature of not lower than 140 DEG C.
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申请公布号 |
US4625064(A) |
申请公布日期 |
1986.11.25 |
申请号 |
US19840597312 |
申请日期 |
1984.04.06 |
申请人 |
TOYO SODA MANUFACTURING CO., LTD. |
发明人 |
KUMOI, SADAKATSU;MITARAI, KEIJI;TSUTSUMI, YUKIHIRO |
分类号 |
C07C217/08;C07C67/00;C07C213/00;(IPC1-7):C07C93/04 |
主分类号 |
C07C217/08 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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