发明名称 SYNTHESIS OF 2-VINYL-4,6-DIAMINO-S-TRIAZINE
摘要 PURPOSE:To produce the titled compound useful as a comonomer, from an inexpensive raw material, easily, in high yield, by reacting 2-[2'-methylimidazolyl (1)']-ethyl-4,6-diamino-S-triazine with epichlorohydrin. CONSTITUTION:The compound of formula III is produced by reacting 2-[2'-methylimidazolyl(1)']-ethyl-4,6-diamino-S-triazine of formula I with epichlorohyrin of formula II in an aqueous solution under heating. Concretely, the raw materials composed of 1mol of the compound of formula I , 1mol of epichlorohydrin of formula II, a small amount of a polymerization inhibitor and a proper amount of water are heated and refluxed for 30min under agitation. The product is cooled, and the obtained product is subjected to conventional recrystallization procedure to obtain the objective substance.
申请公布号 JPS60181076(A) 申请公布日期 1985.09.14
申请号 JP19840036691 申请日期 1984.02.27
申请人 SHIKOKU KASEI KOGYO KK 发明人 SAWA NATSUO;MASUDA TAKESHI
分类号 C07D251/18;C07D403/06 主分类号 C07D251/18
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