摘要 |
PURPOSE:To produce the titled compound useful as a comonomer, from an inexpensive raw material, easily, in high yield, by reacting 2-[2'-methylimidazolyl (1)']-ethyl-4,6-diamino-S-triazine with epichlorohydrin. CONSTITUTION:The compound of formula III is produced by reacting 2-[2'-methylimidazolyl(1)']-ethyl-4,6-diamino-S-triazine of formula I with epichlorohyrin of formula II in an aqueous solution under heating. Concretely, the raw materials composed of 1mol of the compound of formula I , 1mol of epichlorohydrin of formula II, a small amount of a polymerization inhibitor and a proper amount of water are heated and refluxed for 30min under agitation. The product is cooled, and the obtained product is subjected to conventional recrystallization procedure to obtain the objective substance.
|