发明名称 METHOD OF PREVENTING DISTILLATION COLUMN FROM SCALING IN THE CUMENE PHENOL PROCESS
摘要 PURPOSE:Water is added to the crude hydrocarbon recovery fraction which is obtained by air-oxidation of cumene followed by sodium hydroxide treatment to extract organic sodium salts into the aqueous phase, thus collecting phenol without scaling in the distillation column. CONSTITUTION:The oily feed 1, which is obtained by air-oxidation of cumene and treating the product with sodium hydroxide, is combined with water 2. Then, they are mixed by means of a line mixer 3 to extract organic sodium salts into the aqueous phase, subsequently the solid substances are removed with a filter 4 and the water in the emulsion form is settled and separated in the oil- water separator 5, then drained from the line 7. The resultant hydrocarbon recovery fraction is fed through line 6 to the distillation column 8 for hydrocarbon recovery where distillation is effected to collect the objective compound.
申请公布号 JPS60123433(A) 申请公布日期 1985.07.02
申请号 JP19830229072 申请日期 1983.12.06
申请人 MITSUI TOATSU KAGAKU KK 发明人 KINOSHITA YOUZOU;OONO YUKIO;KOSHIBE MINORU;MATSUO HIDEKI
分类号 B01D3/00;C07C1/00;C07C7/04;C07C15/073;C07C15/085;C07C15/44;C07C27/00;C07C37/08;C07C37/70;C07C39/04;C07C67/00 主分类号 B01D3/00
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