发明名称 |
Process for the preparation of 2-cyanomethycyclohexanone. |
摘要 |
<p>@ The invention relates to a process for the preparation of 2-cyanomethylcyclohexanone by
<UnorderedLists id="ula01" listStyle="none"><ListItem>1. converting cyclohexanone to a Mannich base with a secondary amine salt and formaldehyde</ListItem><ListItem>2. converting the Mannich base to the corresponding cyanohydrin with a cyanide</ListItem><ListItem>3. pyrolysing the cyanohydrin obtained in step 2 wherein</ListItem></UnorderedLists>
the pyrolvsis of the cyanohydrin is carried out in the presence of a polar, aprotic solvent having a boiling point of more than 140 °C and/or sodium cyanide.</p> |
申请公布号 |
EP0141449(A1) |
申请公布日期 |
1985.05.15 |
申请号 |
EP19840201328 |
申请日期 |
1984.09.14 |
申请人 |
STAMICARBON B.V. |
发明人 |
CASTELIJNS, ANNA MARIA CORNELIA F.;AARTS, THOMAS MARIA GERARDUS |
分类号 |
C07B61/00;B01J27/00;C07C255/46;B01J27/26;C07C67/00;C07C253/00;(IPC1-7):C07C121/00;C07C120/00 |
主分类号 |
C07B61/00 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|