发明名称 |
Process for preparation of water-free oxide material |
摘要 |
The specification discloses new and improved processes for forming water-free metal or non-metal oxide materials, which may then be melted and formed into optical components in vitreous or crystal form, which are free of the hydrogen-impurity absorption in the near infrared wavelength range. In one process, a water-free oxide is prepared by reacting a chosen nonpolar compound containing the desired metal or non-metal with an aprotic oxygen-containing compound to form the oxide as a precipitate in a chosen aprotic nonaqueous liquid solvent which provides a water-free environment during the formation of the oxide, to prevent the inclusion of water and water-derived impurities in the oxide as formed. Then the oxide-containing precipitate is subjected to a reactive atmosphere process by exposing the powder to a chosen gas phase reactive atmosphere comprising atomic halogen at a predetermined elevated temperature for a predetermined period of time, to remove traces of water and water-derived impurities from the oxide.
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申请公布号 |
US4465656(A) |
申请公布日期 |
1984.08.14 |
申请号 |
US19820481592 |
申请日期 |
1982.04.04 |
申请人 |
HUGHES AIRCRAFT COMPANY |
发明人 |
PASTOR, RICARDO C.;PASTOR, ANTONIO C.;GORRE, LUISA E.;CHEW, REMEDIOS K. |
分类号 |
C01F17/00;C03C1/00;(IPC1-7):C01B33/18;C01G17/02 |
主分类号 |
C01F17/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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