| 摘要 |
An improved method for the production of mercapto functional silanes is provided whereby reactions between haloalkyl silanes and thioureido compounds in the presence of ammonia are accelerated with tertiary nitrogen-containing compounds. In a preferred embodiment the reaction of 3-chloropropyltrimethoxysilane with thiourea is accelerated by N,N-dimethylformamide and other compounds to produce 3-mercaptopropyltrimethoxysilane at lower temperatures and with increased yield.
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