摘要 |
Process for the purification of phosphorus pentasulphide by means of distillation under vacuum at a residual pressure of about 6 mmHg and carried out according to a "thermal profile" comprising, immediately before and immediately after the liquid-vapor-liquid double passage of state, two stationary stages wherein said pentasulphide is maintained in the liquid state at a temperature very close to the boiling temperature of the pentasulphide itself.
|