Process for the manufacture of titanium disulfide

摘要

A process for the manufacture of titanium disulfide by the vapor phase reaction of titanium tetrachloride and a sulfur containing gas. The titanium tetrachloride and the sulfur containing gas are preheated separately and the sulfur containing gas is introduced through a supply conduit at an established rate of flow into a reaction zone and the titanium tetrachloride is introduced into the reaction zone with a downstream component of velocity. A refractory material having a mean particle size greater than the titanium sulfide product is introduced into the product gas stream to impinge on the walls of the reaction zone to eliminate titanium disulfide deposition thereon.