发明名称 Preparation of 5(halophenyl)salicylic acid compounds
摘要 A method of preparing compounds of the formula: <IMAGE> (I.) wherein a novel palladium catalyst system is utilized comprising palladium together with C1-2COO- ligands and halo ligands wherein the molar weight percent based on total ligand molar weight, of the C1-2COO- ligand is from 30 to 60%; and wherein the ratio of the total molar weight of the ligands to the molar weight of palladium utilized is from 4:1 to 10:1; and a catalyst regeneration portion comprising from 0.1 to 8.0 parts of phosphomolybdenovanadic acid per part of palladium catalyst, and at least 20 parts of a solubilizing agent selected from ethylene carbonate, propylene carbonate, and sulfolane, per part of palladium catalyst.
申请公布号 US4237315(A) 申请公布日期 1980.12.02
申请号 US19790090792 申请日期 1979.11.02
申请人 MERCK & CO., INC. 发明人 DOLLING, ULF H.
分类号 C07C65/105;B01J31/00;C07B61/00;C07C51/00;C07C51/09;C07C65/10;C07C67/00;(IPC1-7):C07C65/00 主分类号 C07C65/105
代理机构 代理人
主权项
地址