发明名称 PRODUCTION OF ALKOXYSILANE
摘要 PROBLEM TO BE SOLVED: To obtain the subject compound in the presence of a catalyst industrially obtained at a low cost at a high reaction rate and in a high synthesis yield by reacting metal silicon with a specific alkyl alcohol in the presence of a specific catalyst in an inactive reaction solvent. SOLUTION: This method for producing an alkoxysilane comprises reacting (A) granular metal silicon preferably having a purity of >=80% and an average granule diameter of >=2 mm with (B) a 1-4C alkyl alcohol (e.g. methanol) in the presence of (C) a catalyst (e.g. cuprous chloride produced by a dry method) activated in a linear alkylbenzene together with the component A preferably at 100-350 deg.C in (D) an inactive reaction solvent. Concretely, for example, a linear alkyl benzene, the component A and a catalyst are charged in a reactor, and subsequently heated to activate the catalyst (component C). The component A is reacted with the component B blown into the reactor in the presence of the activated catalyst in the linear alkylbenzene as the component D.
申请公布号 JPH1121288(A) 申请公布日期 1999.01.26
申请号 JP19970192058 申请日期 1997.07.03
申请人 TOAGOSEI CO LTD 发明人 YAMADA YOSHINORI;HARADA MASAYOSHI
分类号 B01J27/122;B01J38/02;C07B61/00;C07F7/04 主分类号 B01J27/122
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