发明名称 PRODUCTION METHOD FOR POLYTHIOL COMPOUND, POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL AND USE THEREFOR
摘要 Provided is a method for producing a polythiol compound, comprising: a step for reacting 2-mercaptoethanol with an epihalohydrin compound represented by the following formula (1) at a temperature of 10°C to 50°C to obtain a polyalcohol compound represented by the following formula (2); a step for reacting the polyalcohol compound thus obtained with thiourea in the presence of hydrogen chloride to obtain an isothiuronium salt; a step for adding, while maintaining a reaction solution containing the isothiuronium salt thus obtained at a temperature of 15°C to 60°C, aqueous ammonia to the reaction solution within 80 minutes, thereby hydrolyzing the isothiuronium salt to obtain a polythiol compound represented by the following formula (5) ; and a step for adding hydrochloric acid which is a concentration of 25% to 36% to the solution containing the polythiol compound thus obtained, washing the solution at a temperature of 10°C to 50°C to purify the polythiol compound.
申请公布号 EP3093282(A1) 申请公布日期 2016.11.16
申请号 EP20160171686 申请日期 2013.02.28
申请人 MITSUI CHEMICALS, INC. 发明人 KAWAGUCHI, MASARU;NISHIMURA, TAKESHI
分类号 C07C319/20;C07C321/14;C08G18/38;C08G75/00;G02B1/04 主分类号 C07C319/20
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