发明名称 PROCESS FOR THE MONOACYLATION OF AMINOHYDROXYNAPHTHALENESULPHONIC ACIDS WITH 2,4,6- TRIFLUORO-S-TRIAZINE
摘要 <p>PROCESS FOR THE MONOACYLATION OF AMINOHYDROXYNAPHTHALENESULPHONIC ACIDS WITH 2,4,6-TRIFLUORO-S-TRIAZINE Process for producing compounds of the formula (1) wherein R is hydrogen, methyl or ethyl, and n is 1 or 2, which process comprises condensing aminohydroxynaphthalenesulphonic acids of the formula (2) with 2,4,6-trifluoro-s-triazine, in an aqueous solution or suspension, within a pH range which is defined by PKN(R)H ? pH ? (pKOH - 2) wherein PKN(R)H and pKOH are the pK values respectively of the amino group and hydroxyl group of the aminohydroxynaphthalenesulphonic acid and pH is the hydrogen exponent, to give compounds of the formula (1).</p>
申请公布号 CA1085394(A) 申请公布日期 1980.09.09
申请号 CA19770289019 申请日期 1977.10.19
申请人 CIBA-GEIGY AG 发明人 BONOMETTI, EMIL;SEILER, HERBERT
分类号 C07D251/44;C09B62/08;C09B62/085;(IPC1-7):07D251/44 主分类号 C07D251/44
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