发明名称 |
METHOD FOR PREPARING THIADIAZOLYLAMIDE COMPOUNDS |
摘要 |
<p>Disclosed is a method for preparing thiadiazolylamide compounds. 2-sulfinyl-5-(trifluoromethyl)-1,3,4-thiadiazole (II) and 2-sulfuryl--5- (trifluoromethyl)-1,3,4-thiadiazole (II') are mixed in mass ratio of 99:1-1:99 as mixed raw materials, and then the mixed raw materials and compound (III) are reacted in the solution of solvent and inorganic base at the temperature of -20-25 ℃ to obtain compound (I). The method disclosed by the invention is simple in the preparation of the mixed raw materials, convenient to operate, high in reaction speed and yield, less in 'three wastes', and suitable for industrial production.</p> |
申请公布号 |
WO2015074180(A1) |
申请公布日期 |
2015.05.28 |
申请号 |
WO2013CN87416 |
申请日期 |
2013.11.19 |
申请人 |
ORIENTAL (LUZHOU) AGROCHEMICALS. CO., LTD.;ZHEJIANG ZHUJI UNITED CHEMICALS CO., LTD. |
发明人 |
SU, YEHUA;CAI, GUOPING;FU, XUEHUA;LIU, WEI;LI, YISHENG;CHEN, BANGCHI |
分类号 |
C07D285/13 |
主分类号 |
C07D285/13 |
代理机构 |
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代理人 |
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