| 摘要 |
FIELD: chemistry.SUBSTANCE: invention relates to a method of obtaining 3-hetaryl-1,5,3-dithiazocinanes, which consists in the interaction of N,N,N,N-tetramethyl -2,6-dithiaheptane -1,7-diamine with hetarylamine in the presence of a catalyst CuClin a molar ratio N,N,N,N-tetramethyl -2,6-dithiaheptane -1,7-diamine:hetarylamine:CuCl=10:10:(0.3-0.7) at a temperature of 55-65°C and atmospheric pressure in chloroform as a solvent for 60-90 min. The output of respective 3-hetaryl-1,5,3-dithiazocinanes constitutes 68-90%..EFFECT: method improvement.1 tbl, 16 ex |
