发明名称 METHOD FOR PRODUCING N-ALKYLBORAZINE
摘要 PROBLEM TO BE SOLVED: To provide a method for producing a borazine compound, with which the reaction yield and the purity of the end product are further improved.SOLUTION: A reaction is conducted by supplying raw material slurry to be added including one of a metal borohydride or an amine salt represented by (RNH)X (in formula, R represents a hydrogen atom, an alkyl group, or a cycloalkyl group, X represents a sulfate group or a halogen atom, and n is 1 or 2) and a solvent to an initially prepared liquid including the other of the metal borohydride and the amine salt and the solvent in a reaction vessel via a feed nozzle 120a. Here, a tip of the feed nozzle is located at a position within a range, corresponding to a distance Lfrom the liquid level of the reaction liquid, of 30-100% of a maximum distance Lin the vertical direction from the liquid level to the inside upper face of the reaction vessel, and the tip of the feed nozzle is located in a region with a similarity ratio of a horizontal plane including the tip of the feed nozzle to the horizontal cross-sectional shape of the reaction vessel of 0-0.8 when the center of gravity of the cross-sectional shape is set to be a center of similitude.
申请公布号 JP2014080376(A) 申请公布日期 2014.05.08
申请号 JP20120227392 申请日期 2012.10.12
申请人 NIPPON SHOKUBAI CO LTD 发明人 KAMIYAMA TAKUYA;MIZUSHIMA CHIHO
分类号 C07F5/05 主分类号 C07F5/05
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