发明名称 |
Method for preparing exo-tricyclo[4.2.1.02,5]non-7-ene-3-spiro-1'-(3'-ethyl-3'-alumina)cyclopentane |
摘要 |
The invention relates to the field of organic synthesis, more specifically to a method for preparing novel organo-aluminum compounds. The compound in question can be used as a component in catalytic systems in processes for the oligomerization and polymerization of olefin, diene and acetylene hydrocarbons as well as in fine organic and organometallic synthesis. The essence of the method consists in reacting 3-methylene-exo-tricyclo[4.2.1.02,5]non-7-ene with triethylaluminium in the presence of the catalyst zirconocene dichloride in an inert gas atmosphere, preferably in argon or nitrogen, at room temperature, in an aliphatic or aromatic solvent for 5-7 h.
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申请公布号 |
US8530688(B2) |
申请公布日期 |
2013.09.10 |
申请号 |
US201013320295 |
申请日期 |
2010.05.13 |
申请人 |
DZHEMILEV USEIN MEMETOVICH;DIYAKONOV VLADIMIR ANATOLIEVICH;TRAPEZNIKOVA OLGA ALEXANDROVNA;IBRAGIMOV ISKHAT GABDRAKHMANOVICH;UCHREZHDENIE ROSSIISKOI AKADEMII NAUK INSTITUT NEFTEKHIMII I KATALIZA RAN |
发明人 |
DZHEMILEV USEIN MEMETOVICH;DIYAKONOV VLADIMIR ANATOLIEVICH;TRAPEZNIKOVA OLGA ALEXANDROVNA;IBRAGIMOV ISKHAT GABDRAKHMANOVICH |
分类号 |
C07F5/06 |
主分类号 |
C07F5/06 |
代理机构 |
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代理人 |
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地址 |
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