发明名称 PROCESS FOR PRODUCING AMINOALKYLTHIOSULFURIC ACID COMPOUND
摘要 An aminoalkylthiosulfuric acid compound represented by formula (1): is produced. In step (A1), a hydrochloride of a chloroalkylamine compound represented by formula (2): is reacted with an alkali metal salt of thiosulfuric acid in the presence of 2 to 6 parts by weight of water with respect to 1 part by weight of the hydrochloride between 50° C. and 100° C. R1 and R2 each represents a hydrogen atom and the like, and n represents an integer of 2 to 9. In step (B1), a mixture of a solid containing the aminoalkylthiosulfuric acid compound and a liquid containing an alkali metal chloride is obtained by adjusting the temperature of the mixture of step (A1) to between -15° C. and 50° C. In step (C1), the aminoalkylthiosulfuric acid compound is obtained as solid by separating the solid containing the aminoalkylthiosulfuric acid compound and the liquid containing the alkali metal chloride from the mixture of (B1).
申请公布号 US2013116468(A1) 申请公布日期 2013.05.09
申请号 US201113808945 申请日期 2011.07.22
申请人 OZTURK ORHAN;SUMITOMO CHEMICAL COMPANY, LIMITED 发明人 OZTURK ORHAN
分类号 C07C381/04 主分类号 C07C381/04
代理机构 代理人
主权项
地址