发明名称 PROCESS FOR PRODUCING 2-ISOPROPENYL-5-METHYL-4-HEXENE-1-YL-3-METHYL-2-BUTENOATE
摘要 Provided is a method capable of solving the problems associated with production of LVSA, which is a pheromone produced by female pest mealybugs, and is useful as an agrochemical pest, at an industrial large scale, and producing LVSA in a high yield. Specifically, the present invention provides a production method of 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate, comprising reacting senecioic acid with a halogenating agent to give senecioic acid halide, reacting the obtained senecioic acid halide with 2-isopropenyl-5-methyl-4-hexen-1-ol in the presence of an organic base compound and heat treating the obtained crude 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate in the presence of a basic substance at 50-250° C.
申请公布号 US2010063314(A1) 申请公布日期 2010.03.11
申请号 US20070519417 申请日期 2007.03.28
申请人 KURARAY CO., LTD. 发明人 UJITA KATSUJI;SAEKI KEISUKE
分类号 C07C69/52 主分类号 C07C69/52
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