发明名称 RECOVERY OF PHENOL LIGANDS DURING THE PRODUCTION OF ISOPULEGOL
摘要 The present invention relates to a method of working up an aluminum-containing reaction product from the production of isopulegol by cyclization of citronellal in the presence of complex compounds, comprising at least one ligand of the formula (I), where R1, R2, R3 are chosen from hydrogen, halogen, nitro, C1-C8-alkyl, C1-C8-alkoxy, di(C1-C4-alkyl)amino and aryl; R4, R5 are chosen from halogen, nitro, C1-C8-alkyl, C1-C8-alkoxy, di(C1-C4-alkyl)amino, aryl or heteroaryl; in which a) the reaction product is subjected to distillative separation to obtain an isopulegol-enriched top product and an isopulegol-depleted bottom product and b) the ligand of the formula (I) is separated off from the bottom product. Moreover, the invention relates to a method of producing isopulegol, and to a method of producing menthol.
申请公布号 EP2059493(A1) 申请公布日期 2009.05.20
申请号 EP20070803135 申请日期 2007.08.31
申请人 BASF SE 发明人 HEYDRICH, GUNNAR;GRALLA, GABRIELE;EBEL, KLAUS;FRIEDRICH, MARKO
分类号 C07C29/17;B01J31/02;B01J31/14;B01J31/40;C07C29/56;C07C29/80;C07C35/12;C07C35/17 主分类号 C07C29/17
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