发明名称 Method for preparing organic ligand-capped titanium dioxide nanocrystals
摘要 The present invention belongs to a method for preparing organic ligand-capped titanium dioxide nanocrystals, wherein the method comprises steps of using methyl titanate, ethyl titanate, n-propyl titanate, iso-propyl titanate, butyl titanate or titanium tetrachloride as a titanium source, and with capping by oleic acid or an organic capping agent, reacting the titanium source in an organic non-polar solvent with an aqueous alkaline substance solution in the interface at a temperature of 25 to 280° C. for 0.5 to 240 hrs, thus a transparent sol containing titanium dioxide nanocrystals is obtained, said the titanium dioxide nanocrystals have particle diameters of 1-20 nm. The preparing process has the features of mild reaction conditions and is a simpler and easier method with a shorter preparation period, thereby facilitating the industrialization.
申请公布号 US2006188431(A1) 申请公布日期 2006.08.24
申请号 US20050293694 申请日期 2005.12.02
申请人 发明人 PAN DAOCHENG;ZHAO NANA;WANG QIANG;JI XIANGLING;JIANG SHICHUN;AN LIJIA
分类号 C01G25/02;C01G23/047;C01G23/053;C09C1/36;C09C1/38;C09C3/08 主分类号 C01G25/02
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