发明名称 METHOD FOR PURIFYING CYCLOPENTENOLONES
摘要 PROBLEM TO BE SOLVED: To provide a method in which thermally unstable cyclopentenolones are simply and effectively purified to a high-purity product, and are advantageously purified in terms of operability and cost effectiveness when implemented in an industrial scale. SOLUTION: The method for purifying cyclopentenolones comprises reacting cyclopentenolones (1) represented by general formula (1), wherein R<SP>1</SP>denotes alkyl, alkenyl, alkynyl or aralkyl; and R<SP>2</SP>denotes hydrogen or alkyl, with calcium chloride in the presence of an ester solvent, separating and obtaining a resultant cyclopentenolones (1)-calcium chloride adduct, and decomposing the adduct to recover cyclopentenolones (1). COPYRIGHT: (C)2003,JPO
申请公布号 JP2003246762(A) 申请公布日期 2003.09.02
申请号 JP20020047712 申请日期 2002.02.25
申请人 SUMITOMO CHEM CO LTD 发明人 MAEHARA AKIRA;SAKAI KIYOMI
分类号 C07C45/85;C07C49/707;(IPC1-7):C07C45/85 主分类号 C07C45/85
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