发明名称 Method for producing fluoroaryl metal compound
摘要 A method for easily and inexpensively producing and purifying a fluoroaryl metal compound such as bis(pentafluorophenyl)dialkyltin which is less colored and has no impurities is provided. Hydrocarbon magnesium halide is reacted with fluoroaryl halide in a solvent including an ether solvent so as to obtain fluoroaryl magnesium halide, which is then reacted with an organic metal compound so as to produce a fluoroaryl metal compound. Tin is more preferable as a metal atom included in the organic metal compound. As for the ether solvent, chain ether solvents are preferable, more specifically, diisopropyl ether, dibutyl ether, and t-butylmethyl ether are more preferable. Besides, it is preferable that magnesium halide, which is a by-product of the fluoroaryl metal compound, is precipitated and removed, or treated with an acid.
申请公布号 US6465668(B2) 申请公布日期 2002.10.15
申请号 US20010993892 申请日期 2001.11.27
申请人 NIPPON SHOKUBAI CO., LTD. 发明人 IKENO IKUYO;MITSUI HITOSHI;IIDA TOSHIYA;MORIGUCHI TOSHIMITSU
分类号 C07F7/22;(IPC1-7):C07F7/22;C07F7/02;C07F7/30 主分类号 C07F7/22
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