| 摘要 |
Provided is a method for purifying a cyanate at high yield from a cyanate crude product solution comprising a cyanate represented by the general formula (1), unsubstituted phenol and non-alcoholic solvent by contacting with a poor solvent containing an alcohol and water, to crystallize the cyanate:in the formula (1), A1 to A3 each independently represents a hydrogen atom or an alkyl group having 1 to 6 carbon atoms; X represents a single bond, an organic group having 1 to 20 carbon atoms, a carbonyl group, a sulfone group, a divalent sulfur atom or oxygen atom; n represents an integer of 0 to 3; and i1 to i3 each independently represents an integer of 0 to 4. And also provided is a method for separating alcohol from non-alcoholic solvent effectively.
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