发明名称 METHOD OF SILYLATION OF INORGANIC OXIDES, AND HIGHLY APOLAR PYROGENIC SILICIC ACID PREPARED BY THIS METHOD
摘要 FIELD: inorganic compounds production. SUBSTANCE: superfine inorganic oxides are treated by at least one silylation reagent poor-volatile within overall process temperature range, silylation reagent being added as liquid in the form of superfine aerosol with drop size less than 500 mcm. Resultant highly apolar pyrogenic silicic acid is characterized by average particle size less than 100 nm, carbon level at least 1 wt % per 100 sq.m/g specific surface (according to BET method), methanol index at least 50, relative hydroxide ion absorption capacity below 25%, lack of soluble and extractable with silicic acid fractions of organosilicon compound, and no isolate silanol groups observed in IR spectra at 3750 cm wavenumber. Product is adequate for use as thickener in polar systems, as absorbent for lubricant oils, as agent improving flowability of toners, and as component of antifoaming agents. EFFECT: improved consumer's properties. 12 cl, 3 tbl, 44 ex
申请公布号 RU2137712(C1) 申请公布日期 1999.09.20
申请号 RU19950109149 申请日期 1995.05.31
申请人 VAKER-KHEMI GMBKH. 发明人 KHERBERT BARTEL';MARIO KHAJNEMANN;FRANTS KHERRMANN;AUGUST AL'TENBUKHNER
分类号 C01B33/18;B01D19/04;C01B13/14;C09C1/30;C09C3/12;C09D7/00;C09K3/32;C11D3/00;C11D3/12;(IPC1-7):C01B33/18 主分类号 C01B33/18
代理机构 代理人
主权项
地址