发明名称 PRODUCTION OF 2,3,5,6 -TETRACHLOROPYRIDINE
摘要 A novel, simple, high-yield process for the production of 2,3,5,6-tetrachloropyridine comprises reacting an ester of 2,2,4-trichloro-4-cyanobutyric acid with excess phosphorus oxychloride in the presence of a catalytic amount of hydrogen chloride and optionally in the presence of an aprotic inert solvent, at a temperature of 100-160 .degree.C, preferably at 120-140 .degree.C for about 5-10 hours, under elevated pressure, if necessary.
申请公布号 CA2170778(C) 申请公布日期 1999.04.27
申请号 CA19942170778 申请日期 1994.09.02
申请人 发明人 SHVO, YOUVAL
分类号 C07D213/61;(IPC1-7):C07D213/61 主分类号 C07D213/61
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