发明名称 |
LIQUID PHTHALIC ANHYDRIDE RECOVERY PROCESS |
摘要 |
A process for recovering phthalic anhydride as a liquid from a vapor phase oxidation product which comprises mixing the vapor phase oxidation product having a temperature in the range of about 130 DEG C or greater with a first stream comprising maleic anhydride and/or at least one compound selected from the group consisting of: citraconic anhydride, benzoic acid and phthalic anhydride in a rectification tower such that a substantial portion of the phthalic anhydride contained within the vapor phase oxidation product transfers from the vapor phase to a liquid phase and the by-products contained in the first stream which are more volatile than phthalic anhydride transfer from the liquid phase to the vapor phase and wherein a vapor-to-liquid weight ratio in the range between about 5 to 20 is exhibited within the rectification tower, thereby forming a liquid phase phthalic anhydride product having a phthalic anhydride concentration in the range between about 50-100 wt.% , preferably 90-100 wt.%, without the formation of an intermediate solid phase.
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申请公布号 |
WO9531427(A1) |
申请公布日期 |
1995.11.23 |
申请号 |
WO1995US05891 |
申请日期 |
1995.05.09 |
申请人 |
EXXON CHEMICAL PATENTS INC. |
发明人 |
DENGLER, HERBERT, PETER;BAIEL, JAMES, JOSEPH |
分类号 |
C07C51/573;(IPC1-7):C07C63/16 |
主分类号 |
C07C51/573 |
代理机构 |
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地址 |
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