A high temperature process for producing alkyllithium compounds in high yields of at least 90% and high purity comprising reacting, in a liquid hydrocarbon solvent, an alkyl halide containing 3 to 16 carbon atoms and mixtures thereof with lithium metal particles of less than 300 microns in size at a temperature between 35 DEG and 125 DEG C. and recovering the alkyllithium compound.
申请公布号
US5332533(A)
申请公布日期
1994.07.26
申请号
US19930087582
申请日期
1993.07.06
申请人
FMC CORPORATION
发明人
SCHWINDEMAN, JAMES A.;MORRISON, ROBERT C.;DOVER, B. TROY;ENGEL, JOHN F.;KAMIENSKI, CONRAD W.;HALL, RANDY W.;SUTTON, DOUGLAS E.