发明名称 |
PROCESS FOR THE PREPARATION OF A PURIFIED ACRYLAMIDO SULFONIC ACID MONOMER DERIVATIVE |
摘要 |
A process for the preparation of a purified monomer is disclosed which comprises the steps of reacting an impure monomer (A) wherein R1 and R2 are independently hydrogen or alkyl groups containing from 1 to about 6 carbon atoms, with (B) a substantially aqueous solution of an oxide or hydroxide of the structure MO or MOH wherein M is a Group IA or Group IIA metal, or an amine of the structure NR3R4R5 wherein R3, R4 and R5 are independently hydrogen or alkyl, alkanol or alkoxy groups containing from 1 to about 12 carbon atoms, wherein the molar ratio of (A):(B) is from about 1:1-2 for Group IA metals, 2:1-2 for Group IIA metals or ratio of moles of (A) to nitrogens of (B) is from about 1:1-2 nitrogens to form a salt, and recovering a purified salt by crystallization by subjecting the aqueous solution to changes in temperature and/or pressure and/or concentration.
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申请公布号 |
CA2087715(A1) |
申请公布日期 |
1992.12.04 |
申请号 |
CA19922087715 |
申请日期 |
1992.05.06 |
申请人 |
LUBRIZOL CORPORATION (THE) |
发明人 |
QUINN, ROBERT E.;BURK, W. MICHAEL;HENRY, WILLIAM S.;GOODLIVE, STEVEN A. |
分类号 |
C07C303/44;C07C309/15;(IPC1-7):C07C309/15 |
主分类号 |
C07C303/44 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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