发明名称 METHOD OF D-RIBOSE PREPARATION
摘要 The solution concerns a preparation of highly pure D-ribose. The 15 to 20 percent water solution of D-arabinose is introduced in contact with ion exchange resin with functional quaternary benzyltrimethylammonium groups, with bound molybdenum ions at a temperature of 90 to 100 degrees C for a period of 4 to 6 hours. The reaction mixture of D-ribose, D-arabinose, D-lyxose, D-xylose is used for preparation of crystalline N-phenyl-D-ribosylamine by means of aromatic amine, from whose hydrolysis by water vapour D-ribose is released. After obtaining D-ribose the mixture of sugars in mother liquor can be chromatographically selectively separated on a column with ion exchange resin with functional sulfo groups, which was modified by univalent, bivalent or trivalent metal using from 40 to 60 percent of water solution of ethanol.
申请公布号 CS274863(B2) 申请公布日期 1991.11.12
申请号 CS19870010305 申请日期 1987.12.31
申请人 CHEMICKY USTAV SAV,CS 发明人 KUBALA JOZEF ING.,CS;BURDATSOVA ANDREA,CS
分类号 C13K3/00;C13K13/00;(IPC1-7):C13K13/00 主分类号 C13K3/00
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