发明名称 Process for the preparation of metallizable azo dyes carrying out coupling in an inert gas atmosphere in the presence of an ammonium salt
摘要 A process for the preparation of an azo dye of formula <IMAGE> (1) wherein K is the beta -naphthol radical, X is hydrogen or nitro and M is an alkali metal ion or an ammonium ion, which process comprises coupling an aqueous solution containing 15 to 30 percent by weight of a diazo component of formula <IMAGE> (2) and 6 to 20 mol % of an ammonium salt, based on the molar amount of the diazo component, at a pH in the range from 10.5 to 11.5 and in an inert gas atmosphere, to a coupling component of formula <IMAGE> (3) in which formulae (2) and (3) above K and X are as defined for formula (1). The present invention makes it possible to obtain the claimed azo dyes in high yield.
申请公布号 US4994561(A) 申请公布日期 1991.02.19
申请号 US19900536054 申请日期 1990.06.08
申请人 CIBA-GEIGY CORPORATION 发明人 JOSWIG, HANS P.;HUBER, WERNER
分类号 C09B29/01;C09B29/15;C09B41/00 主分类号 C09B29/01
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